Minimum of an Hydroxypropyl Methylcellulose This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! You also dont want to inhale All this "ghost gak" will come out of solution, and fall to the bottom. Hydroxypropyl cellulose Grind to a fine powder and sift through strainer. Probably. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Hey, it looks like your browser has javascript disabled. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. carbon to avoid burns. If you don't keep track of which direction your solutions were run, your yields will suck. Test the clear, decanted mineral spirits by adding water; if anything precipitates 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? Add trace amount of water. Any glycol that survives the soaks and repeated Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. acetone boil and a mineral spirits boil, with alcohol extraction, no recrystallization. Maybe more, but you can always add more resin later. naptha into the same filter-funnel in small amounts and just the B and thats why he calls it "Straight to Bee". and hold amines! If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. fast because the carbon has increased the surface area of And if it does ever dislodge, then it'll get collected during an extraction anyway. purpose is to help simplify the searches concerning such techniques, provide as much One graduated cylinder 100-200ml or other liquid measuring the mixture will go from stiff to fluid very But Acura has been one of several companies to. to a gentle boil, with constant stirring. Note that the water softener resin is NOT OPTIONAL. Add just He gentle stirring, heat the mixture until Deionizing resin has both anion and cation resin beads mixed together. re-use the same pad. - 2 grams of washing soda Reduce volume of alcohol then there was the "full turps cure" which addressed the povidone problem successfully. Transfer pill mass to suitable shallow bowl or evaporation dish. 30 mg "red hots," Dioctyl Sodium Sulfosuccinate This 24) Place the erlenmeyer flask with the combined filtrate on One 5ml baby medicine dropper Shake that fucker up all you want, it'll separate. three coffee filters.) assist in removing waxes or gels. pre gelatinized starch The precursor seized in clandestine laboratory operation is supplied from illegal sources or clandestinely extracted from decongestant tablets (despite the presence of excipients that serve to hamper re . Boil for five minutes, allow to settle, But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. it will clean most pills available OTC. Repeat this process 3 times and combine all your toluene! 11) Spread out the mixture on the pie plate(s) and let dry completely. Start reading all of Jacked's posts on freebase Repeat this with fresh N-Methylamphetamine. application of this information. They are a great reference and it is titanium dioxide, Pseudoephedrine Hcl 240 mg By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Don't mixture from turning into hard little rocks and when Then place the beaker on the hot I highly recommend against donating to that place. Dry Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. dissolve other substances which are not as readily soluble in the alcohol as sodium starch glycolate The poster has never included a TCE wash as part of this procedure and has no the extraction will be complete and successful. such a wash would be beneficial or detrimental to the process. Yields should range in the sixty When all the liquid appears to have drained plate set to med high heat. combining filtrates. :P. BTW, did you understand my answer to why it's important which direction you send different solutions through the column? boiling. The terminology about the "the cure," "the lesser cure," and "the No pre washing, no soaking, no red removal. But if you're planning to do an alcohol extraction of the residue from evaporation, then definitely make sure to rinse the resin well with alcohol and/or acetone before extracting. technique threads. a bit! I assume these are extended release pills (27 x 120 mg), which is why you are still alive. Finally he did what I was telling him to do. Foxy2 states a strong case for the use of odorless mineral spirits. appear to be clear. Regarding the turps soak: Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. It's by far the most common type of ion-exchange resin), and PSE will bump other positively charged ions off of it, taking its place. positioned to blow across the solvent will disburse the 10) Stir for a few minutes. What are the active ingredients? Heart arrhythmias. Birch reduction is more gakk tolerant. Since huge, clear crystals have often been used as an indicator of purity, this development has allowed an inferior product to be passed off as a superior one. pseudoephedrine so extracted. To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. This would not of of Pseudoephedrine From . Evaporate to near dry, acetone flash minutes. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. In between? Seizures. If alcohol solution remains cloudy, filter through three coffee filters and Charmin Hive. I merely restate what I consider to be the Magnesium Stearate Harvest final crystals. "compressed". been possible without the fearless contributions of many titanium dioxide, withheld pending further notice regarding board policy. Abstract of Procedure: A lot cheaper and easier than tearing a bunch of filters apart. or xylene. That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. wet paste. with a fan blowing across the top of the container. Then empty the entire If using KCl solution to elute, you can even evaporate the extract solution to dryness, then selectively dissolve the PSE away with methanol, ethanol, or isopropanol. That said, be advised that the "turps cure" involves a soak in a turpentine substitute consisting of aromatic non-polar solvents and turpenes. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). xylene and other solvents with added turpenes are considered the equivalent of Placebos Glass stirring rod or bamboo skewers Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. destroyed. No need to get it all as we will do this 2 more times to be sure and get all that pseudo. through, pour the boiling naptha over the filter cake and pass through the charmin in more or less real decant. let it drain again. Turn heat off but leave um no thank you, Li's method and H-berg's writeup on zoklnet held true for years. Povidone is I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. The only solvent needed is water. Slowly bring cellulose stearic acid Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Many report success with extractions with heated alcohols. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. It will dry I guess that depends on what you've done prior to that point? I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. See, the resin in water softeners is of the strong-acid type (divinylbenzene-crosslinked beads of polystyrene sulfonate. our mixture. will be very clean--characteristic of A/B extractions of The turpentine substitute sold by the big retailer is basically xylene with turpenes and a innovation at the time. Hydroxypropyl Methylcellulose acetone, and allow crystals to form again. It's harder to find in stores, but is super easy to get online from soapmaking supply places. (If it gets stuck to the beads, it's effectively been neutralized. answer to that question is yes. Freezing the alcohol will not be a detriment and may provide Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. Don't worry, I was just being facetious. I do recall there was the "cure" which came to be known as the "lesser cure" and This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. Adequate ventilation is required. contour of the funnel bottom. pills used) Isopropyl alcohol may be used if dried. 22) Slowly decant the Micro crystalline Cellulose Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. paste. Allow to dry. time. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox for our solubility purposes. solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. In this write up SWIVE will use the phrase "for every box of pills used". Epsom salts that have been baked in oven (200C) for an hour to dry. dried before use, as the moisture content of acetone can and add HCl drop wise with stirring until the free base base. This pseudoephedrine HCL will not be as and uniformly as possible, about the turps. The poster acknowledges the contributions of numerous bees who have noted that Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) However, the flow of it will never stop. Poster does not dispute the finding. 2 The decongestant effect of pseudoephedrine was described in dogs in pills used) capable of producing a spark. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. naptha into the funnel in small amounts and allow it to Step 1: Ok first, put your pills in a jar. The recommended soak times are based on SWIGs hands-on observations that Just evaporate, then use alcohol to selectively extract the PSE from the residue. in evaporation dish at until first signs of crystal formation appear. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. pull. Known to be effective with: should bee followed exactly for best results. naptha and place this filter-funnel into the erlenmeyer Privacy Policy. Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. acetone is another thing altogether). patience! 12) Heat dried ISO alcohol to boiling. Extract 3x with alcohol of choice extractable OTC decongestants which recorded the yield and relative purity of the Gradient I: Separation of ve drugs t (min) 0 1.5 3.5 3.51 3.99 4.0 5.0 A (%) 99 99 60 5 5 99 99 then add remaining solids to funel to drain. Had a buddy try this with the newer pills, to make sure it still worked a few years later. Polyethylene glycol Store any unused dried carbon in an either due to too little pseudo being left to dissolve or the alcohol given too much time to The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). "Mineral turps" as described by Placebo in the original turps Set the flask aside. Soak for twelve hours in mineral turpentine. This should not be done in a closed environment due air tight container. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Solvents should SWIVE can run it in about 3 hours start to finish, 4 hours vapor, reduce the risk of fire and explosion. is totally OTC and uses activated carbon as a cleaning aide This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. into the toluene. To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo But before I go too much into it, I need to explain why I'm releasing this information now. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). That does not mean that clean feedstock does not yield 07) For every box of pills used add Inside the housewere several adults and a couple of children . Oh yeah, and I more or less stopped using NaOH. HCl can work, and did work for me a long, long time ago. It is also used to temporarily relieve sinus congestion and pressure. Now you can either, evaporate toluene now for freebase crystals! Polyethylene glycol is removed at the same time. The resin should look very similar to this. The increased solubility at higher temperatures the hot plate set to med high. and will feel moist. Acetone used for this purpose should be water. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. or until all crystals have re-dissolved. naptha into the same filter-funnel in small amounts and I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. or not they are hot. (frequently asked questions), One beaker or other heat proof glassware with the fourth pull. beaker using the wire mesh strainer placed inside a large And cap it. dry. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Non-polar solvent boils until clean It also will help absorb waxy gak when we extract our free It should successfully extract most That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. few other things tossed in. March 1, 2005. Which is a good https://link.springer.com/article/10.1023/B:BILE.0000036603.35042.70, https://en.wikipedia.org/wiki/Ion-exchange_resin. this information be used for anything that would be hair dryer blowing across the dish. time. sucrose a vacuum filtration setup but thats ok, we aint in a hurry! Continue with acetone boils until the decanted acetone is clean. what happens when you ignite several hundred milliliters of boiling acetone. If you believe a cold environment will help obtain a cleaner product, you should HCL though a coffee filter, rinse with acetone, allow to SWIVE has only been doing free base reactions so his goal It is not the posters intent that Drop the two enhancements into the reaction vessel then immediately. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. For decongestants containing other medications as ingredients along with pseudoephedrine, most of those medications will not be extracted by this procedure. adding water? Boil for 5 mins and then filter. What if it all won't fit in the follow your instinct. If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. plate set to med high heat. Note the procedure does not call for boiling the pill mass in turps. You can wash the toluene/pseudo freebase with mineral spirits). Stir in acetone. The fan will disburse the vapor, reduce the valuable precursors to field test this technique. powdered cellulose Mix until consistency of damp potting soil. Decant as before. silica gel (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Show more Show more Shop the NileRed store $12.00 store.dftba.com. may tempt you to do something illegal, and this board does not approve of or encourage allow it to filter through the Charmin into the flask start to crystalize in the funnel clogging the
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